Book excerpt: Metal Oxide-based Nanofibers and their Applications provides an in-depth overview on developments surrounding the synthesis, characterization properties, and applications achieved by scientific leaders in the area. Sections deal with the theoretical and experimental aspects of the synthesis and methodologies to control microstructure, composition and shape of the nanofibrous metal oxides, review the applications of metal oxide nanofibers in diverse technologies, with special focus on the relation between the structural, morphological and compositional features of the nanofibers, cover applications of metal oxide nanofibers in the fields of sensing (biosensing, gas sensing), and consider biomedical and cleaning technologies. Lastly, a final section covers their application in energy generation and storage technologies (e. g. piezoelectric, solar cells, solid oxide fuel cells, lithium-ion batteries, supercapacitors, and hydrogen storage are reviewed. Reviews electrospinning methods for the synthesis and design of nanocomposites and hybrid metal oxide nanofibers Discusses applications of metal oxide nanofibers in sensing, biomedical fields, cleaning technologies, and energy Emphasizes the structural, morphological and compositional properties of nanofibers and their effect on device performance